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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2174436Generated: November 1, 2026

Benzoic acid, 4-amino-, 1,1-dimethylethyl ester → HCID 67627060, compound

https://huagongshe.com/reaction/2174436

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzoic acid, 4-amino-, 1,1-dimethylethyl esterHCID 233272—
ReactantHCID 54679210HCID 54679210—
SolventTolueneHCID 1140—
ProductHCID 67627060HCID 67627060—

Reaction Steps

Ethyl 1-hexyl-4-hydroxy-2-oxo-1,2-dihydroquinoline-3-carboxylate (159 mg, 0.5 mmol) and tert-butyl 4-aminobenzoate (193 mg, 1 mmol) are suspended in anhydrous toluene (4 ml) and are microwave-heated with the container open (the parameters are the following: power=200 W, temperature=120° C., execution time=7 min, hold time=10 min).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09061997B2
Source datasetuspto-grants-2015_06
ORD IDord-e14c7f55c10246e3a69a5024f3539b8c
Source noteuspto-grants-2015_06