HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic acid, 4-amino-, 1,1-dimethylethyl ester → HCID 67627060, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic acid, 4-amino-, 1,1-dimethylethyl ester | HCID 233272 | — |
| Reactant | HCID 54679210 | HCID 54679210 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 67627060 | HCID 67627060 | — |
Reaction Steps
Ethyl 1-hexyl-4-hydroxy-2-oxo-1,2-dihydroquinoline-3-carboxylate (159 mg, 0.5 mmol) and tert-butyl 4-aminobenzoate (193 mg, 1 mmol) are suspended in anhydrous toluene (4 ml) and are microwave-heated with the container open (the parameters are the following: power=200 W, temperature=120° C., execution time=7 min, hold time=10 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09061997B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-e14c7f55c10246e3a69a5024f3539b8c |
| Source note | uspto-grants-2015_06 |