HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2174703Generated: October 29, 2026
Diisopropylethylamine → HCID 59452233, compound
https://huagongshe.com/reaction/2174703
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 45123180 | HCID 45123180 | — |
| Reactant | HCID 58290013 | HCID 58290013 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Solvent | Acetic acid toluene | HCID 18331056 | — |
| Product | HCID 59452233 | HCID 59452233 | — |
Reaction Steps
200.0 μl (10.0 μmol) of a 0.05 molar 2-(5-chloro-thiophen-2-yl)-4,4-dimethyl-4H-oxazol-5-one solution in toluene/acetic acid 9:1 are combined with 200.0 μl (10.0 μmol) of a 0.05-molar 3-cyclopropyl-2,3,4,5-tetrahydro-1H-benzo[d]azepin-7-ylamine solution in DMF and 1.7 μl (10.0 μmol) DIPEA, heated to 80° C. overnight and left to stand for 2 days at room temperature. The reaction solution is filtered through basic aluminium oxide and the filtrate is evaporated down i. vac.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09062034B2 |
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| Source dataset | uspto-grants-2015_06 |
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| ORD ID | ord-49a84130ed814cefb0ef9a5208b38199 |
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| Source note | uspto-grants-2015_06 |
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