HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 86644563, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 68485462 | HCID 68485462 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86644563 | HCID 86644563 | — |
Reaction Steps
A mixture of 0.85 g (2.9 mmol) methyl 1-[(5-chloro-thiophen-2-yl)-carbonylamino]-cyclopent-3-ene-1-carboxylate and 20 ml methylene chloride is combined with 0.92 g 70% meta-chloroperbenzoic acid at 0° C. and stirred for 3 h at room temperature. The mixture is washed with sat. Sodium hydrogen carbonate solution and concentrated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09062034B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-ea0457bc56a34c25b86cdef843491469 |
| Source note | uspto-grants-2015_06 |