Hydrochloric Acid → HCID 67086843, compound

HRID 2174979Notes

Reaction equation

HRID 2174979 reaction equation
C(OC([N:8]1[CH2:14][CH:13]2[CH:9]1[CH2:10][N:11]([C:15]1[CH:24]=[N:23][C:22]3[C:17](=[CH:18][CH:19]=[CH:20][CH:21]=3)[N:16]=1)[CH2:12]2)=O)(C)(C)C.Cl>O1CCOCC1.ClCCl>[CH:13]12[CH2:14][NH:8][CH:9]1[CH2:10][N:11]([C:15]1[CH:24]=[N:23][C:22]3[C:17](=[CH:18][CH:19]=[CH:20][CH:21]=3)[N:16]=1)[CH2:12]2

Participants

5

Reactant 2

HCID 313Hydrochloric AcidHCID 67086542HCID 67086542, compound

Product 1

HCID 67086843HCID 67086843, compound

Reagents, catalysts & solvents 2

HCID 6344DichloromethaneSolventHCID 312751,4-DioxaneSolvent

Procedure

3-Quinoxalin-2-yl-3,6-diaza-bicyclo[3.2.0]heptane-6-carboxylic acid tert-butyl ester (0.52 mmol) was treated with 4M HCl in dioxane (2 mL) in dichloromethane (2 mL) to give the title compound. MS (ESI) mass calcd. for C13H14N4, 226.28; m/z found 227.2 [M+H]+.

Sources & evidence

ORD record
ord-0fda1e86b25f481ebd12d6acb612e28c
Source dataset
uspto-grants-2015_06
Patent number
US09062044B2

Reaction notes

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