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HRID2175008

反应详情

EQUATION

反应方程式

HRID 2175008 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)C(F)(F)F
HCID6422

未命名化合物

结构：CC(C)(C)OC(=O)N1CC[C@@H]2CN(C(=O)OCc3ccccc3)[C@@H]2C1
HCID67086554

未命名化合物

PRODUCTS

生成物

1
结构：O=C(OCc1ccccc1)N1C[C@H]2CCNC[C@H]21
HCID71432745

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

To (1S,6R)-8-benzyl 3-tert-butyl 3,8-diazabicyclo[4.2.0]octane-3,8-dicarboxylate (300 mg, 0.9 mmol) in CH2Cl2 was added TFA (1:1). After 2 h, the reaction was concentrated and used without further purification.

WORKUP

后处理

  1. concentrationthe reaction was concentrated
  2. customused without further purification