HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Fluoro-2-iodobenzoic acid → 4-fluoro-2-(2H-1,2,3-triazol-2-yl)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Fluoro-2-iodobenzoic acid | HCID 13158583 | — |
| Reactant | 5-fluoro-2-(2H-1,2,3-triazol-2-yl)benzoic acid | HCID 67086948 | — |
| Product | 4-fluoro-2-(2H-1,2,3-triazol-2-yl)benzoic acid | HCID 67086886 | — |
Reaction Steps
The title compound was prepared in a manner analogous to Intermediate 41, substituting 4-fluoro-2-iodo-benzoic acid for 5-fluoro-2-iodo-benzoic acid. 1H NMR (400 MHz, CD3OD): 7.93 (s, 2H), 7.88 (dd, J=8.7, 5.9 Hz, 1H), 7.56 (dd, J=9.2, 2.5 Hz, 1H), 7.38-7.30 (m, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09062044B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-7ad9ec04e77d499bb41d7f487e59c26f |
| Source note | uspto-grants-2015_06 |