HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 53250711, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-Chloro-1-propanol | HCID 12313 | — |
| Reactant | HCID 53250560 | HCID 53250560 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53250711 | HCID 53250711 | — |
Reaction Steps
88 mg (0.25 mmol) of 1-[6-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)pyridin-2-yl]piperazine are irradiated in the microwave at 140° C. for 2 h with 42 μl (0.50 mmol) of 3-chloropropan-1-ol in 2 ml of ethanol and 70 μl (0.50 mmol) of triethylamine. The reaction mixture is evaporated and purified by means of preparative HPLC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09062015B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-6c2c8a8a87f442ed9a7be57949601ed5 |
| Source note | uspto-grants-2015_06 |