HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67607456, compound → HCID 68331159, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67607456 | HCID 67607456 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68331159 | HCID 68331159 | — |
Reaction Steps
52 mg (0.11 mmol) of 6-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)-3′,6′-dihydro-2′H-2,4′-bipyridinyl-1′-carboxylic acid tert-butyl ester are dissolved in 20 ml of ethanol and hydrogenated using a Pd/C cartridge (10%, 30×4 mm) in an H Cube (Thales Nanotechnology). The solvent is subsequently distilled off.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09062015B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-f3a66f3ea8934bd099bfe5c19b14331d |
| Source note | uspto-grants-2015_06 |