Hydrochloric Acid → HCID 67247956, compound

HRID 2175108Notes

Reaction equation

HRID 2175108 reaction equation
C(OC([N:8]1[CH2:14][CH2:13][CH2:12][CH:11]([NH:15][CH2:16][CH2:17][CH2:18][CH2:19][OH:20])[CH2:10][CH2:9]1)=O)(C)(C)C.Cl>O1CCOCC1>[NH:8]1[CH2:14][CH2:13][CH2:12][CH:11]([NH:15][CH2:16][CH2:17][CH2:18][CH2:19][OH:20])[CH2:10][CH2:9]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 67257525HCID 67257525, compound

Product 1

HCID 67247956HCID 67247956, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent2×

Procedure

The product from step b (1.32 g, 4.65 mmol) is dissolved in 8 ml of dioxane, 16 ml of 4N HCl in dioxane are added, and the mixture is stirred at RT overnight. The reaction mixture is evaporated and dried under high vacuum.

Workup

  1. customThe reaction mixture is evaporated
  2. customdried under high vacuum

Sources & evidence

ORD record
ord-f0414dc7bf6e489dbc2164e5ccd354ca
Source dataset
uspto-grants-2015_06
Patent number
US09062015B2

Reaction notes

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