Hydrochloric Acid → HCID 58562799, compound

Participants

Reaction Steps

A solution of N-(1-(1,4-dioxaspiro[4.5]decan-8-yl)allyl)-2-methylpropane-2-sulfinamide (1.38 g, 4.58 mmol), prepared in the previous step, was dissolved in methanol (100 mL) and treated with HCl (15 mL. 18.7 mmol, 1.25 M in MeOH), stirring overnight at room temperature. The reaction mixture was concentrated in vacuo, triturated with ether, decanting the supernatant several times and the residue dried under high vacuum afford the product as a white foam (HCl salt).

Provenance & Evidence