HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86727040, compound → HCID 89633271, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86727040 | HCID 86727040 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 89633271 | HCID 89633271 | — |
Reaction Steps
To a solution of the title compound of Step D ((0.46 g, 0.88 mmol) in methanol (30 mL) was added palladium on carbon (10%, 0.094 g, 0.088 mmol) and the mixture was subjected to hydrogenation at rt overnight. After filtration the filtrate was concentrated to give the title compound. LC/MS: (M+1)+: 388.10.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09062070B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-b32272001023467e9af099a0b7eb4050 |
| Source note | uspto-grants-2015_06 |