HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 71270731, compound → HCID 86727107, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 71270731 | HCID 71270731 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86727107 | HCID 86727107 | — |
Reaction Steps
A mixture of ethyl 3-nitro-6,7-dihydro-5H-cyclopenta[b]pyridine-7-carboxylate (4.2 g, 17.8 mmol) and Pd/C (0.5 g, 10%) in 80 mL of ethanol was stirred at room temperature under 50 psi of hydrogen for 2 hours then filtered. The filtrate was concentrated to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09062070B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-058cbfafeec940d7ac097bbd727a210a |
| Source note | uspto-grants-2015_06 |