HuagongsheHuagongshe Chemistry Print Report · For research reference only
ethyl 3-(2H-1,2,3-triazol-2-yl)quinoline-2-carboxylate → 3,6'-Dimethyl-[2,3'-bipyridine]-2'-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | ethyl 3-(2H-1,2,3-triazol-2-yl)quinoline-2-carboxylate | HCID 90411115 | — |
| Reactant | Methyl 3,6'-dimethyl-[2,3'-bipyridine]-2'-carboxylate | HCID 90412135 | — |
| Product | 3,6'-Dimethyl-[2,3'-bipyridine]-2'-carboxylic acid | HCID 90412565 | — |
Reaction Steps
Prepared analogous to intermediate A-33 step B substituting ethyl 3-(2H-1,2,3-triazol-2-yl)quinoline-2-carboxylate with the title compound of step D. MS (ESI) mass calcd. for C13H12N2O2, 228.2; m/z found 229 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09062078B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-da06dbb7ee854a6fb1f1896453363d60 |
| Source note | uspto-grants-2015_06 |