Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 90412485 | HCID 90412485 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 90411401 | HCID 90411401 | — |
Reaction Steps
To the title compound from step A (300 mg, 1 mmol) in 1,4-dioxane (3 mL) was added 6N HCl in iPrOH (1 mL). The reaction was heated to 70° C. for 3 h, cooled to rt and concentrated to give the title compound that was used without further purification. MS (ESI) mass calcd. for C11H15N3O, 205.1; m/z found 206.0 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09062078B2 |
|---|
| Source dataset | uspto-grants-2015_06 |
|---|
| ORD ID | ord-fe9ff343efd24e1984fcf36ddd9f905e |
|---|
| Source note | uspto-grants-2015_06 |
|---|
