Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 90411801 | HCID 90411801 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 90413940 | HCID 90413940 | — |
Reaction Steps
To the title compound of Step A (91 mg, 0.5 mmol) in EtOH (1 mL) was added 4M KOH (0.5 μL). The reaction was then heated at 90° C. for 18 h. The reaction was then cooled to rt, acidified with 1N HCl (aq) to pH=3, concentrated and used without further purification in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09062078B2 |
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| Source dataset | uspto-grants-2015_06 |
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| ORD ID | ord-2aedd6f016fc447a96e9355a486875d0 |
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| Source note | uspto-grants-2015_06 |
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