Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 90411630 | HCID 90411630 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 90413051 | HCID 90413051 | — |
Reaction Steps
To the title compound from step A (343 mg, 1 mmol) in 1,4-dioxane (10 mL) was added 6N HCl in iPrOH (1 mL). The reaction was heated to 70° C. for 2 h, cooled to rt, concentrated and used without further purification in subsequent steps.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09062078B2 |
|---|
| Source dataset | uspto-grants-2015_06 |
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| ORD ID | ord-89daacb7ed8640e48ff452cd6c1fd81b |
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| Source note | uspto-grants-2015_06 |
|---|