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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2175977Generated: October 31, 2026

Hydrochloric Acid → HCID 90413051, compound

https://huagongshe.com/reaction/2175977

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 90411630HCID 90411630—
SolventIsopropanolHCID 3776—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 90413051HCID 90413051—

Reaction Conditions

Temperature70 °C

Reaction Steps

To the title compound from step A (343 mg, 1 mmol) in 1,4-dioxane (10 mL) was added 6N HCl in iPrOH (1 mL). The reaction was heated to 70° C. for 2 h, cooled to rt, concentrated and used without further purification in subsequent steps.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09062078B2
Source datasetuspto-grants-2015_06
ORD IDord-89daacb7ed8640e48ff452cd6c1fd81b
Source noteuspto-grants-2015_06