HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 90370137, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | Methyl 6-methylpyrazine-2-carboxylate | HCID 13153470 | — |
| Product | HCID 90370137 | HCID 90370137 | — |
Reaction Steps
By using 3.42 g of methyl 6-methylpyrazine-2-carboxylate and 4.40 g of NBS, a bromination reaction was performed by the method similar to Preparation Example 62. Thereafter, by using 10 mL of morpholine as amine, the reaction similar to Preparation Example 9 was performed, thereby obtaining 987 mg of methyl 6-(morpholin-4-ylmethyl)pyrazine-2-carboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09062032B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-30fb0a6af9c84d4e9cb3e4b9415d4e84 |
| Source note | uspto-grants-2015_06 |