1-Bromo-4-fluorobenzene → HCID 11694956, compound

HRID 2176105Notes

Reaction equation

HRID 2176105 reaction equation
[C:1](=[N:14][NH2:15])([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Br[C:17]1[CH:22]=[CH:21][C:20]([F:23])=[CH:19][CH:18]=1>>[C:2]1([C:1]([C:8]2[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=2)=[N:14][NH:15][C:17]2[CH:22]=[CH:21][C:20]([F:23])=[CH:19][CH:18]=2)[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 99931-Bromo-4-fluorobenzeneHCID 79304Diphenylmethylidenehydrazine

Product 1

HCID 11694956HCID 11694956, compound

Procedure

General procedure A was used to convert benzophenone hydrazone (1.962 g, 10.0 mmol; Aldrich) and 1-bromo-4-fluorobenzene (1.75 g, 10.0 mmol; source) to the title compound. MS (DCI/NH3) m/z 291 (M+H)+.

Sources & evidence

ORD record
ord-8c924ec0aa334ee68c83539ffe9f543f
Source dataset
uspto-grants-2015_06
Patent number
US09063126B2

Reaction notes

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