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HRID21764

反应详情

EQUATION

反应方程式

HRID 21764 的结构方程式

REACTANTS

反应物

2
结构：[Al+3].[H-].[H-].[H-].[H-].[Li+]
HCID21226445

未命名化合物

结构：CC(C=C[C@@H]1CCCN1C(=O)OCc1ccccc1)=NO
HCID86748737

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc([C@@H]2CCCN2C)on1
HCID119380

3-Methyl-5-(1-methyl-2(S)-pyrrolidinyl)isoxazole

C9H14N2O

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

The Cbz-protected compound of step 23d is reacted with LAH in THF at 0° C. as described in Example 24 below, and the title compound is isolated in pure form by extraction with ethyl acetate and distillation under high vacuum.