HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3,4-Trimethoxybenzoic acid → HCID 68276482, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3,4-Trimethoxybenzoic acid | HCID 11308 | — |
| Reactant | (3aS,4R,7aS)-4-hydroxy-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester | HCID 68276168 | — |
| Product | HCID 68276482 | HCID 68276482 | — |
Reaction Steps
Synthesis in analogy to the General Method 1 starting from (3aS,4R,7aS)-4-hydroxy-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester and 2,3,4-trimethoxy-benzoic acid to yield (3aR,4S,7aR)-4-m-tolylethynyl-4-(2,3,4-trimethoxy-benzoyloxy)-octahydro-indole-1-carboxylic acid methyl ester. MS [M+H]=296 (ester elimination ion); RT=8.527 min; HPLC Method I
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09067881B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-fc7a1fade4a642079bbcae134fb8af0e |
| Source note | uspto-grants-2015_06 |