HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Acetamidopyridine-4-carboxylic acid → HCID 60141331, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Acetamidopyridine-4-carboxylic acid | HCID 3774466 | — |
| Reactant | (3aS,4R,7aS)-4-hydroxy-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester | HCID 68276168 | — |
| Product | HCID 60141331 | HCID 60141331 | — |
Reaction Steps
Synthesis in analogy to the General Method 1 starting from (3aS,4R,7aS)-4-hydroxy-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester and 2-acetylamino-isonicotinic acid to yield (3aR,4S,7aR)-4-(2-acetylamino-pyridine-4-carbonyloxy)-4-m-tolylethynyl-octahydro-indole-1-carboxylic acid methyl ester. MS [M+H] 476; RT=7.443 min HPLC Method I
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09067881B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-14361df054864b88bb6d19445297ac53 |
| Source note | uspto-grants-2015_06 |