HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanogen Bromide → HCID 58136895, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanogen Bromide | HCID 10476 | — |
| Reactant | HCID 86650807 | HCID 86650807 | — |
| Product | HCID 58136895 | HCID 58136895 | — |
Reaction Steps
(6-Chloro-5-cyclopropylpyridazin-3-yl)hydrazine trifluoroacetic acid salt (W3.012; 400 mg) was converted and worked up analogously to W2.008, except that, instead of 0.5, one further equivalent of cyanogen bromide solution was added. 260 mg of the title compound were obtained in sufficient purity.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08198272B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-d273ced451b04d0d86ab05ee44004f0d |
| Source note | uspto-grants-2012_06 |