HRID2177624

反应详情

EQUATION

反应方程式

HRID 2177624 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of 3-nitro-N-phenylpyridin-4-amine (20 g, 93 mmol) in MeOH (500 mL) was added 10% Pd/C. The reaction was stirred under a hydrogen atmosphere for 10 h. The reaction was filtered and the filtrate was concentrated to afford the product (17.2 g, 100%).

WORKUP

后处理

  1. filtrationThe reaction was filtered
  2. concentrationthe filtrate was concentrated