HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluoroaniline → 1-(4-fluorophenyl)-7-methyl-1H-[1,2,3]triazolo[4,5-c]pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluoroaniline | HCID 9731 | — |
| Reactant | 2-Aminopyridine | HCID 10439 | — |
| Reactant | 4-Chloro-3-nitropyridine | HCID 2735781 | — |
| Reactant | 4-Chloro-3-methyl-5-nitropyridine | HCID 58882371 | — |
| Product | 1-(4-fluorophenyl)-7-methyl-1H-[1,2,3]triazolo[4,5-c]pyridine | HCID 90409692 | — |
Reaction Steps
The title compound was prepared in a manner analogous to Intermediate 17, Step 1 through Intermediate 19, Step 3 substituting 4-chloro-3-methyl-5-nitro-pyridine for 4-chloro-3-nitropyridine and 4-fluoroaniline for 2-aminopyridine in the synthesis of Intermediate 17, Step 1. MS (ESI) mass calcd. C12H9FN4, 228.1. m/z found, 229.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09066946B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-64d4e4e8d90f4377ba776133b40a2492 |
| Source note | uspto-grants-2015_06 |