HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2177641Generated: October 30, 2026
HCID 90409398, compound → HCID 90409551, compound
https://huagongshe.com/reaction/2177641
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 90409398 | HCID 90409398 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 90409551 | HCID 90409551 | 92.3% |
Reaction Steps
The product of Example 238, Step 3 (90 mg, 0.22 mmol) was dissolved in a solution of HCl in dioxane (4M, 2 mL). The reaction was heated at 90° C. for 16 h. The solvent was removed in vacuo to afford the title compound (50 mg, 92%). MS (ESI) mass calcd. C13H15FN4, 246.10; m/z found, 247.16 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09066946B2 |
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| Source dataset | uspto-grants-2015_06 |
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| ORD ID | ord-05d5592fc33c4806adf19ee49ba81df2 |
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| Source note | uspto-grants-2015_06 |
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