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HRID2177676

反应详情

EQUATION

反应方程式

HRID 2177676 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：COC(=O)c1c(CS(=O)(=O)c2ccccc2)ccc(-c2ccoc2)c1OCCN(C)C
HCID67107506

未命名化合物

2 次

PRODUCTS

生成物

1
结构：CN(C)CCOc1c(-c2ccoc2)ccc(CS(=O)(=O)c2ccccc2)c1C(=O)O.Cl
HCID52914642

未命名化合物

PROCEDURE

实验过程

Prepared by proceeding in a similar manner to Example 3, starting from methyl 6-(benzenesulphonylmethyl)-2-(2-dimethylaminoethoxy)-3-(furan-3-yl)benzoate (Intermediate 17). The product after chromatography was treated with hydrochloric acid (1M) and then evaporated to dryness. The residue was triturated with ether and the solid was collected by filtration.

WORKUP

后处理

  1. customPrepared
  2. customevaporated to dryness
  3. customThe residue was triturated with ether
  4. filtrationthe solid was collected by filtration