HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Z)-methyl 6-((2-(3-(diethylamino)prop-1-enyl)-4-fluorobenzenesulfonyl)methyl)-3-(furan-3-yl)-2-methoxybenzoate → Ethyl 6-(benzenesulphonylmethyl)-3-(furan-3-yl)-2,4-dimethoxybenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Z)-methyl 6-((2-(3-(diethylamino)prop-1-enyl)-4-fluorobenzenesulfonyl)methyl)-3-(furan-3-yl)-2-methoxybenzoate | HCID 69915014 | — |
| Reactant | HCID 86677123 | HCID 86677123 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Ethyl 6-(benzenesulphonylmethyl)-3-(furan-3-yl)-2,4-dimethoxybenzoate | HCID 86677122 | — |
Reaction Steps
Prepared by proceeding in a similar manner to Intermediate 160, starting from ethyl 6-(benzenesulphonylmethyl)-3-iodo-2,4-dimethoxybenzoate (Intermediate 201), using THF instead of dioxane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09067905B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-bb5f62407e5443e3abd9496eec4a69b5 |
| Source note | uspto-grants-2015_06 |