HRID2178112

反应详情

EQUATION

反应方程式

HRID 2178112 的结构方程式

PROCEDURE

实验过程

The title compound was prepared according to the method described for Method Variation 1 using 3-cyano-4-fluoro-N-(5-fluoropyridin-2-yl)benzenesulfonamide (Preparation 2) and 3-chloro-2-fluoro-5-hydroxypyridine and then purified using silica gel column chromatography eluting with 30-35% EtOAc in heptanes.

WORKUP

后处理

  1. custompurified
  2. washeluting with 30-35% EtOAc in heptanes