HRID2178130

反应详情

EQUATION

反应方程式

HRID 2178130 的结构方程式

PROCEDURE

实验过程

The title compound was prepared according to the method described for Preparation 11 using N-(2,4-dimethoxybenzyl)-5-fluoropyridin-2-amine (Preparation 20) and 4-fluoro-5-bromobenzenesulfonyl chloride at 40° C. The residue was purified by silica gel column chromatography eluting with 10% EtOAc in heptanes.

WORKUP

后处理

  1. customThe residue was purified by silica gel column chromatography
  2. washeluting with 10% EtOAc in heptanes