HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 67953983, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 67953948 | HCID 67953948 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67953983 | HCID 67953983 | — |
Reaction Steps
To a solution of compound 10-F (0.066 g, 0.084 mmol) in methylene chloride (2 mL) was added trifluoroacetic acid (1 mL) and the resulting mixture was stirred at room temperature overnight. The solvent was evaporated in vacuo and the crude product, isolated as a light yellow oil, was used in the next step without further purification; MS m/z (M+H+) 356.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09067935B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-379308ba10a241a284f144ec763e0318 |
| Source note | uspto-grants-2015_06 |