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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2178664Generated: October 30, 2026

Hydrazine hydrate (1:1) → HCID 68380694, compound

https://huagongshe.com/reaction/2178664

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrazine hydrate (1:1)HCID 24654—
Reactant4-Fluoro-1,3-benzothiazol-7-olHCID 68379869—
SolventEthanolHCID 702—
ProductHCID 68380694HCID 68380694—

Reaction Conditions

Temperature80 °C

Reaction Steps

A solution of 4-fluoro-1,3-benzothiazol-7-ol (C14) (2.02 g, 11.93 mmol) in ethanol (20 mL) was treated with hydrazine monohydrate (12.7 mL, 167 mmol) and stirred for at 80° C. for 1 hour. The reaction was concentrated in vacuo and used directly in the following step.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09067934B2
Source datasetuspto-grants-2015_06
ORD IDord-66a30ca9923e4a488453bab305543965
Source noteuspto-grants-2015_06