HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 55238268, compound → 2-(1H-pyrazol-1-yl)-5-(trifluoromethyl)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 55238268 | HCID 55238268 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-(1H-pyrazol-1-yl)-5-(trifluoromethyl)aniline | HCID 7064033 | 48% |
Reaction Steps
Method C3 was used 1-(2-nitro-4-(trifluoromethyl)phenyl)-1H-pyrazole (1.80 g, 7.00 mmol) in EtOH (40 mL) to give 760 mg (48%) of the title compound as white crystals after crystallization from hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08198279B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-379a0809e0d646d786bfcacd8767ffe3 |
| Source note | uspto-grants-2012_06 |