HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(2-Bromoacetyl)pyridine hydrobromide → HCID 71575799, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(2-Bromoacetyl)pyridine hydrobromide | HCID 2776234 | — |
| Reactant | HCID 89586134 | HCID 89586134 | — |
| Reactant | HCID 178441789 | HCID 178441789 | — |
| Product | HCID 71575799 | HCID 71575799 | — |
Reaction Steps
In analogy to the procedure described for the synthesis of 2-[5-tert-Butyl-7-(3,3-difluoro-pyrrolidin-1-yl)-[1,2,3]triazolo[4,5-d]pyrimidin-2-yl]-1-(2-chloro-phenyl)-ethanone (example 47), the title compound was prepared from 5-tert-butyl-7-(3,3-difluoropyrrolidin-1-yl)-3H-[1,2,3]triazolo[4,5-d]pyrimidine and 2-bromo-1-(pyridin-3-yl)ethanone hydrobromide and isolated as light yellow solid. MS (m/e): 402.3 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09067943B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-53a94e687dba4c5a84cb71cb3eff77d4 |
| Source note | uspto-grants-2015_06 |