HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Aminopropyl)triethoxysilane → 2-(6-Hydroxy-3-oxo-3H-xanthen-9-yl)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Aminopropyl)triethoxysilane | HCID 13521 | — |
| Reactant | Fluorescein 5-isothiocyanate | HCID 18730 | — |
| Solvent | (+-)-2-Butanol | HCID 6568 | — |
| Product | 2-(6-Hydroxy-3-oxo-3H-xanthen-9-yl)benzoic acid | HCID 3383 | — |
| Product | Silane | HCID 23953 | — |
Reaction Steps
50 μl APS (γ-amino propyltriethoxyl silane) and 1 ml FITC (fluorescein isothiocyanate, 1 mg/ml ethanol solution) are added into a 4 ml absolute ethyl ethanol under obturation condition to react for 12 hours, so as to obtain a precursor solution upon coupling of fluoresceine and silane coupling agent. The method for preparing the precursor solution is common knowledge in prior art. 3.65 ml ethanol/water mixture (ratio of ethanol to water is 8), 1.2 ml ethanol and 100
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09068084B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-b356f3e9bd554eda81e0356cf5b4ce32 |
| Source note | uspto-grants-2015_06 |