HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroformate → HCID 73207753, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | HCID 73207834 | HCID 73207834 | — |
| Reactant | HCID 73207857 | HCID 73207857 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 73207753 | HCID 73207753 | 43.1% |
Reaction Steps
Ethyl chloroformate (300 μmol; 28 μl) is added to a solution of the compound of Example 9 (100 μmol; 40 mg) in pyridine (0.5 ml). The reaction mass is stirred for 2 hours then treated in the same manner as for the preparation of the compound of Example 17. 20 mg of product is obtained in the form of a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06887869B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-40eac1d7e427410ea8c63f69b0b54737 |
| Source note | uspto-grants-2005_05 |