HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131724852, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 85051032 | HCID 85051032 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 131724852 | HCID 131724852 | 65.2% |
Reaction Steps
A solution of hydrochloric acid (0.3 mmol; 0.3 ml; 1N in ether) is added to a solution of the compound of Example 16 (0.22 mmol; 100 mg) in acetone (2 ml). The precipitate is filtered, washed with a little acetone, with ether and dried under reduced pressure. 70 mg of the expected product is obtained in the form of a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06887869B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-ed9fda5824734000861599dc9385680f |
| Source note | uspto-grants-2005_05 |