HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131724853, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 85336862 | HCID 85336862 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 131724853 | HCID 131724853 | 84.5% |
Reaction Steps
A solution of hydrochloric acid (0.8 mmol; 0.8 ml; 1N in ether) is added to a solution of the compound of Example 29 (0.44 mmol; 196 mg) in acetone (4 ml). The precipitate is filtered, washed with a little acetone, with ether and dried under reduced pressure. 180 mg of the expected product is obtained in the form of a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06887869B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-3ac911f59f954970ad3ec37e4b448092 |
| Source note | uspto-grants-2005_05 |