HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2,4-Dichlorobenzotrifluoride → gamma-[5-Chloro-2-(trifluoromethyl)phenoxy]-N-methylbenzenepropanamine hydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2,4-Dichlorobenzotrifluoride | HCID 9443 | — |
| Edukt | tert-Butyl (3-hydroxy-3-phenylpropyl)carbamate | HCID 15431788 | — |
| Edukt | 4-Chloro-5-fluoro-2-{[(1R)-3-iodo-1-phenylpropyl]oxy}benzonitrile | HCID 69798650 | — |
| Produkt | gamma-[5-Chloro-2-(trifluoromethyl)phenoxy]-N-methylbenzenepropanamine hydrochloride | HCID 22489955 | — |
Reaktionsschritte
The title compound was prepared by the method of Example 3 (b) using racemic (3-hydroxy-3-phenylpropyl)carbamic acid 1,1-dimethylethyl ester and 2,4-dichloro-1-(trifluoromethyl)benzene to give 70 mg of the product as a colourless solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06887871B2 |
| Quelldatensatz | uspto-grants-2005_05 |
| ORD ID | ord-7cedfcb1980240f7875e2129062b5824 |
| Quellennotiz | uspto-grants-2005_05 |