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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2179976Generated: October 30, 2026

HCID 86759701, compound → HCID 69800369, compound

https://huagongshe.com/reaction/2179976

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86759701HCID 86759701—
SolventHydrochloric AcidHCID 313—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 69800369HCID 69800369155.1%

Reaction Steps

The product from step (c) (370 mg, 0.9 mmol) was dissolved in 4M hydrochloric acid in dioxan and stirred at room temperature for a half hour. The solvent was removed in vacuo and the residue triturated with a mixture of ethyl acetate and methanol (14:1). The white solid was filtered and dried to afford the title compound (243 mg, 70%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06887871B2
Source datasetuspto-grants-2005_05
ORD IDord-9984bde08fea498a8cd56203fb971db2
Source noteuspto-grants-2005_05