HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86759701, compound → HCID 69800369, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86759701 | HCID 86759701 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 69800369 | HCID 69800369 | 155.1% |
Reaction Steps
The product from step (c) (370 mg, 0.9 mmol) was dissolved in 4M hydrochloric acid in dioxan and stirred at room temperature for a half hour. The solvent was removed in vacuo and the residue triturated with a mixture of ethyl acetate and methanol (14:1). The white solid was filtered and dried to afford the title compound (243 mg, 70%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06887871B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-9984bde08fea498a8cd56203fb971db2 |
| Source note | uspto-grants-2005_05 |