HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 90745477, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 4-Chloro-2,5-difluorobenzonitrile | HCID 11275302 | — |
| Reactant | HCID 91232705 | HCID 91232705 | — |
| Product | HCID 90745477 | HCID 90745477 | 78.4% |
Reaction Steps
The product from step (a) (0.1 g) and 2,5-difluoro-4-chloro-benzonitrile (0.18 g) and sodium hydride (60% dispersion in oil, 0.035 g) were subjected to the procedure described in Example 90(a) to afford the product as a gum (0.15 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06887871B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-c87904dda8f2462a86c26e4457249220 |
| Source note | uspto-grants-2005_05 |