HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 60003043, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 87973066 | HCID 87973066 | — |
| Product | HCID 60003043 | HCID 60003043 | — |
Reaction Steps
Following General Procedure G, ethyl 7-(7-ethoxy-4-ethyl-2,2-dimethyl-2H-chromen-6-yl)-3-methyl-octa-2E,4E,6Z-trienoate (Compound 35,23 mg, 0.058 mmol) was hydrolyzed with 1M NaOH. Purification by column chromatography (silica gel, 30% ethyl acetate in hexanes) followed by recrystallization from acetonitrile gave rise to the title compound as a light yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06887896B1 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-7678877f4a414dec857e7c6bf4ed95ce |
| Source note | uspto-grants-2005_05 |