HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl morpholine oxide → (2E)-3-(7-Ethoxy-2,2-dimethyl-4-phenyl-2H-chromen-6-yl)-2-fluoro-but-2-enal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl morpholine oxide | HCID 82029 | — |
| Reactant | HCID 22490895 | HCID 22490895 | — |
| Product | (2E)-3-(7-Ethoxy-2,2-dimethyl-4-phenyl-2H-chromen-6-yl)-2-fluoro-but-2-enal | HCID 22490763 | — |
Reaction Steps
Following General Procedure M, (2E)-3-(7-ethoxy-2,2-dimethyl-4 phenyl-2H-chromen-6-yl)-2-fluoro-but-2-en-1-ol (Compound 88, 137 mg, 0.37 mmol) and 4-methylmorpholine N-oxide (87 mg, 0.74 mmol) were reacted to give the title compound as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06887896B1 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-0aa4e4454ce1422abc9af2e4a950e2c6 |
| Source note | uspto-grants-2005_05 |