HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 4-(diethoxyphosphoryl)-3-methylbut-2-enoate → HCID 131724861, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 4-(diethoxyphosphoryl)-3-methylbut-2-enoate | HCID 6000084 | — |
| Reactant | HCID 22490769 | HCID 22490769 | — |
| Product | HCID 131724861 | HCID 131724861 | — |
Reaction Steps
Following General Procedure O, ethyl 4-(diethoxyphosphoryl)-3-methyl-but-2E-enoate (230 mg, 0.84 mmol) and (2E)-3-(7-ethoxy-4-isopropyl-2,2-dimethyl-2H-chromen-6-yl)-2-fluoro-but-2-enal (Compound 98, 96 mg, 0.29 mmol) were reacted to give the title compound as a yellow oil after purification by column chromatography (silica gel, 5% ethyl acetate in hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06887896B1 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-776216f478f4469fb62780916edb8d0b |
| Source note | uspto-grants-2005_05 |