HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminumhydride → HCID 22490980, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminumhydride | HCID 21225700 | — |
| Reactant | HCID 86597841 | HCID 86597841 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22490980 | HCID 22490980 | — |
Reaction Steps
Following General Procedure G-1, diisobutylaluminum hydride (1.0 M in hexanes, 2.2 mL, 2.2 mmol) and ethyl (2E)-2-fluoro-3-(4,4-dimethyl-6-ethoxy-1-isopropyl-3,4-dihydronaphthalen-7-yl)-2-butenoate (Compound A-43, 0.205 g, 0.55 mmol) in THF (6 mL) were reacted to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06887896B1 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-5248750ad53546a2ba77052d589e886a |
| Source note | uspto-grants-2005_05 |