Diisobutylaluminumhydride → HCID 22490882, compound

Participants

Reaction Steps

As described in General Procedure G-1, ethyl (2E)-2-fluoro-3-(4,4-dimethyl-6(cyclopropyl)methoxy-1-iso-propyl-3,4-dihydronaphthalen-7-yl)-2-butenoate (Compound A-45, 0.025 g, 0.062 mmol) and diisobutylaluminum hydride (1.0 M in hexanes, 0.50 mL, 0.50 mmol) were reacted in THF (0.5 mL) to produce the title compound as an oil.

Provenance & Evidence