Diisobutylaluminumhydride → HCID 22490808, compound

Participants

Reaction Steps

As described in General Procedure G-1, ethyl (2E)-2-fluoro-3-(4,4 dimethyl-6-ethoxy-1-tert-butyl-3,4-dihydronaphthalen-7-yl)-2-butenoate (Compound A-46, 0.037 g, 0.095 mmol) and diisobutylaluminum hydride (1.0 M in hexanes, 0.76 mL, 0.76 mmol) were reacted in THF (0.75 mL) to produce the title compound as an oil.

Provenance & Evidence