HRID2180575
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
As described in General Procedure G-1, ethyl (2E)-2-fluoro-3-(4,4 dimethyl-6-n-propoxy-1-tert-butyl-3,4-dihydronaphthalen-7-yl)-2-butenoate (Compound A-48, 0.044 g, 0.109 mmol) and diisobutylaluminum hydride (1.0 M in hexanes, 0.87 mL, 0.87 mmol) were reacted in THF (0.87 mL) to produce the title compound as an oil.