HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl morpholine oxide → HCID 86597845, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl morpholine oxide | HCID 82029 | — |
| Reactant | HCID 69731067 | HCID 69731067 | — |
| Product | HCID 86597845 | HCID 86597845 | — |
Reaction Steps
Following General Procedure H-1, (2E)-3-(3-ethoxy-5,5-dimethyl-5,6-dihydro-naphthalen-2-yl)-2-fluoro-pent-2-en-1-ol (Compound A-50, 35 mg, 0.12 mmol) and 4-methylmorpholine N-oxide (27 mg, 0.23 nmol) were reacted to give the title compound as a yellow solid after purification by flash chromatography (silica gel, 10% ethyl acetate in hexanes).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06887896B1 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-f73cde027d424cce80f67ad1455a18cd |
| Source note | uspto-grants-2005_05 |