HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid methylene chloride → HCID 11818309, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Reactant | 4(1H)-Quinazolinone | HCID 135408753 | — |
| Product | HCID 11818309 | HCID 11818309 | — |
Reaction Steps
100 mg of resin (7) is suspended in 2 ml of a 50% trifluoroacetic acid/methylen chloride solution and shaken for 1.5 hours at room temperature. Customary working up for solid-phase reactions afforded 3-(3-aminopropyl)-2-phenyl-3H-quinazolin-4-one;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06890930B1 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-5d018b0faa3743b48f291368ca1604fb |
| Source note | uspto-grants-2005_05 |