L-Methionine → HCID 69796973, compound

Participants

Reaction Steps

7.27 g (4RS,5RS)-5-(4-chlorobenzyl)-4-dimethylaminomethyl-2,3,4,5-tetrahydrobenzo[b]oxepin-5-ol were reacted with 43 ml methanesulfonic acid and 4.81 g methionine analogously to the procedure described in example 6. After similarly analogous working up, separation of the product and salt formation, the title compounds were obtained in the form of white crystals.

Provenance & Evidence